background removed
calibration : 1- XAS energy reference from standard similar LSMO (maximum of MnL3 peak)
2- energy dispersion calibration of the detector from two peaks reference in low and core loss areas (STO substrate area in the multimayer system).
see also TiL3 Analyst: imhoff. Temperature: Room.
Use in HyperSpy
import exspy
spectra = exspy.data.eelsdb(title="strontium titanate", formula="SrTiO3")
s = next(sp for sp in spectra if sp.original_metadata.json.id == 21741)
s.plot(plot_edges=True)
Specimen
Formula
SrTiO3
Elements
Sr, Ti, O
Edges
O K
Source and purity
STO substrate (perovskite multilayers UMP CNRS-Thales Palaiseau France)
Energy range
519.17 – 562.02 eV
Step
0.242 eV
Keywords
imported from old site
Treatment
Dark current corrected
Yes
Gain variation corrected
No
Acquisition
Microscope
STEM-VG
Gun
Cold FEG
Beam energy
100 kV
Convergence semi-angle
7 mrad
Collection semi-angle
22 mrad
Mode
STEM
Detector
Parallel: 666 + CCD modified Orsay
Probe size
0.7 nm²
Integration time
0.3 s
Readouts
10
Reference
EELS study of interfaces in magnetoresistive LSMO/STO/LSMO tunnel junctions
Samet L., Imhoff D., Maurice J-L., Contour J-P., Gloter A., Manoubi T., Fert A., Colliex C.,
European-Physical-Journal-B., 34(2), 179-92, 2003