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Melamine Powder -Irradiated

Core loss C3N6H6 · Susana Trasobares · added 2007-11-19 · Beam energy and angles known · History

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The experiment was performed with the chronospectroscopy mode, every spectrun was acquired using an acquisition time of 9 millisecond. The submitted spectrum is a collection of 10 spectra. Melamine is really sensitive to beam damage, after 0.4 seconds the origianl melamine spectra is transformed into the spectrun submitted here. Analyst: Susana Trasobares. Temperature: Room.

Use in HyperSpy
import exspy

spectra = exspy.data.eelsdb(title="Melamine Powder -Irradiated", formula="C3N6H6")
s = next(sp for sp in spectra if sp.original_metadata.json.id == 21628)
s.plot(plot_edges=True)

Specimen

Formula
C3N6H6
Elements
C, N, H
Edges
C K
Source and purity
Aldrich 99%
Energy range
244.41 – 457.19 eV
Step
0.208 eV

Keywords

  • imported from old site

Treatment

Dark current corrected
Yes
Gain variation corrected
Yes

Acquisition

Microscope
VG HB501
Gun
Cold FEG
Beam energy
100 kV
Convergence semi-angle
15 mrad
Collection semi-angle
24 mrad
Monochromated
No
Detector
Parallel: 666 Gatan
Probe size
0.5 nm²

Reference

Susana Trasobares, Christine Kolczewski, Riitta Räty, Niclas Borglund, Arianna Bassan, Gilles Hug, Christian Colliex, Stefan Csillag, Lars G. M. Pettersson. “Monitoring the Decomposition of Melamine in the Solid Phase by Electron Energy Loss Chronospectroscopy”. J. Phys. Chem. A, 107(2), 228-235 (2003). doi:10.1021/jp026340j Article

Other links

Please cite this spectrum

If you use this spectrum, cite the contributor's paper and the EELS Data Base.

Susana Trasobares. Melamine Powder -Irradiated (C3N6H6). EELS Data Base, spectrum 21628, 2007. https://eelsdb.eu/spectra/melamine-powder-irradiated/

Susana Trasobares, Christine Kolczewski, Riitta Räty, Niclas Borglund, Arianna Bassan, Gilles Hug, Christian Colliex, Stefan Csillag, Lars G. M. Pettersson. “Monitoring the Decomposition of Melamine in the Solid Phase by Electron Energy Loss Chronospectroscopy”. J. Phys. Chem. A, 107(2), 228-235 (2003). doi:10.1021/jp026340j

Philip Ewels, Thierry Sikora, Virginie Serin, Chris P. Ewels and Luc Lajaunie. “A Complete Overhaul of the Electron Energy-Loss Spectroscopy and X-Ray Absorption Spectroscopy Database: eelsdb.eu.” Microscopy and Microanalysis 22, 717–724 (2016). doi:10.1017/S1431927616000179
BibTeX
@misc{Trasobares2007eelsdb21628,
  author = {Susana Trasobares},
  title = {Melamine Powder -Irradiated},
  howpublished = {EELS Data Base, spectrum 21628},
  year = {2007},
  url = {https://eelsdb.eu/spectra/melamine-powder-irradiated/}
}

@article{Trasobares2007eelsdb21628ref,
  author = {Susana Trasobares, Christine Kolczewski, Riitta Räty, Niclas Borglund, Arianna Bassan, Gilles Hug, Christian Colliex, Stefan Csillag, Lars G. M. Pettersson},
  title = {Monitoring the Decomposition of Melamine in the Solid Phase by Electron Energy Loss Chronospectroscopy},
  journal = {J. Phys. Chem. A},
  volume = {107},
  number = {2},
  pages = {228--235},
  year = {2003},
  doi = {10.1021/jp026340j}
}

@article{ewels2016eelsdb,
  author = {Ewels, Philip and Sikora, Thierry and Serin, Virginie and Ewels, Chris P. and Lajaunie, Luc},
  title = {A Complete Overhaul of the Electron Energy-Loss Spectroscopy and X-Ray Absorption Spectroscopy Database: eelsdb.eu},
  journal = {Microscopy and Microanalysis},
  volume = {22},
  pages = {717--724},
  year = {2016},
  doi = {10.1017/S1431927616000179}
}
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