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Graphite (really glassy carbon)

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- Energy Axis is not calibrated, CCD point spread function has long tails,these have not be corrected for.- The ratio of the pi*/sigma* peaks depends on sample orientation (See Leapman and Silcox, PRL, V42, 1361 (1979)).- Note 0.7 eV split Analyst: David Muller (at Cornell University) 1995. Temperature: Room. BEAM/Crystal: parallel to c-axis.

Use in HyperSpy
import exspy

spectra = exspy.data.eelsdb(title="Graphite (really glassy carbon)", formula="C (graphite)")
s = next(sp for sp in spectra if sp.original_metadata.json.id == 21547)
s.plot(plot_edges=True)

Specimen

Formula
C (graphite)
Elements
C
Edges
C K
Source and purity
Combined test specimen, imaged parallel to c-axis of graphite particle
Energy range
269.75 – 313.9 eV
Step
0.088 eV

Keywords

  • imported from old site

Treatment

Dark current corrected
Yes
Gain variation corrected
No

Acquisition

Microscope
VG HB501A
Gun
Cold FEG
Beam energy
100 kV
Convergence semi-angle
18 mrad
Collection semi-angle
16 mrad
Resolution
0.5 eV
Mode
STEM
Detector
GIF:
Probe size
0.3 nm²
Beam current
0.12
Integration time
10 s
Readouts
15

Other links

Please cite this spectrum

If you use this spectrum, cite the contributor and the EELS Data Base.

David Muller. Graphite (really glassy carbon) (C (graphite)). EELS Data Base, spectrum 21547, 2005. https://eelsdb.eu/spectra/graphite-really-glassy-carbon/

Philip Ewels, Thierry Sikora, Virginie Serin, Chris P. Ewels and Luc Lajaunie. “A Complete Overhaul of the Electron Energy-Loss Spectroscopy and X-Ray Absorption Spectroscopy Database: eelsdb.eu.” Microscopy and Microanalysis 22, 717–724 (2016). doi:10.1017/S1431927616000179
BibTeX
@misc{Muller2005eelsdb21547,
  author = {David Muller},
  title = {Graphite (really glassy carbon)},
  howpublished = {EELS Data Base, spectrum 21547},
  year = {2005},
  url = {https://eelsdb.eu/spectra/graphite-really-glassy-carbon/}
}

@article{ewels2016eelsdb,
  author = {Ewels, Philip and Sikora, Thierry and Serin, Virginie and Ewels, Chris P. and Lajaunie, Luc},
  title = {A Complete Overhaul of the Electron Energy-Loss Spectroscopy and X-Ray Absorption Spectroscopy Database: eelsdb.eu},
  journal = {Microscopy and Microanalysis},
  volume = {22},
  pages = {717--724},
  year = {2016},
  doi = {10.1017/S1431927616000179}
}