- An arbitrary background was subtracted, because no one know the exact background behind a ionisation edge. Therefore, I do not want to say the absolute intensities are right, but due to the low frequency of EXELFS oscilations.- Calibration could not be accurate Analyst: Stefan Nufer.
Use in HyperSpy
import exspy
spectra = exspy.data.eelsdb(title="Aluminium oxide alpha", formula="Al2O3 (alpha)")
s = next(sp for sp in spectra if sp.original_metadata.json.id == 21578)
s.plot(plot_edges=True)
Specimen
Formula
Al2O3 (α)
Elements
Al, O
Edges
Al L1
Source and purity
single crystal
Energy range
112.9 – 172.9 eV
Step
0.1 eV
Keywords
imported from old site
Treatment
Dark current corrected
No
Gain variation corrected
No
Thickness
0.2 t/λ
Acquisition
Microscope
VG HB501UX
Gun
cold field emission
Beam energy
100 kV
Convergence semi-angle
10 mrad
Collection semi-angle
6.5 mrad
Resolution
0.8 eV
Mode
STEM
Detector
Parallel:
Probe size
1 nm²
Beam current
1
Reference
Stefan Nufer, Thomas Gemming, Christian Elsaesser, Sibylle Koestlmeier, Manfred Ruehle, Ultramicroscopy, 86, 339, 2001